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• W4387668830 abstract "We have explored possible reasons for oval-shaped electron diffraction ring patterns instead of regular ring patterns (so-called Debye–Scherrer rings) observed in single particles of layered manganese dioxide (hexagonal birnessite, K0.33MnO2) that contains K cations in between the MnO2 slabs. Atomic-resolution scanning transmission electron microscopy observations along in-plane directions have revealed that the interlayer K cations are arranged with a tripled periodicity in the in-plane direction, while the stacking periodicity of the interlayer K cations in the out-of-plane (c-axis) direction was partially lost. Such a structure with a one-dimensional disorder has been successfully described on the basis of the order–disorder (OD) theory. In addition to the one-dimensional disorder in stacking of the interlayer K cations, a high density (approximately 0.5 nm–1) of stacking faults of the MnO2 slabs along the c-axis exist. Each stacking disorder (interlayer K stacking and MnO2 slab stacking) produces diffuse diffraction streaks on the systematic rows of superlattice and fundamental reflections, respectively. On top of that, each particle consists of layered domains of approximately 20 nm thickness, which are randomly rotated with respect to each other while maintaining the common c-axis (c-axis texture). Owing to the combined effects of the two types of stacking disorder and c-axis texture, the reciprocal lattice of single particles of K0.33MnO2 becomes concentric columnar walls. The oval diffraction ring patterns can be considered the consequence of the intersection of the concentric columnar reciprocal lattice and the Ewald sphere (approximated as a plane)." @default.
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• W4387668830 date "2023-10-16" @default.
• W4387668830 modified "2023-10-17" @default.
• W4387668830 title "Dual Origin of Oval Diffraction Rings in K-Containing Layered Manganese Dioxide" @default.
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• W4387668830 doi "https://doi.org/10.1021/acs.jpcc.3c05881" @default.
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