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- W44473336 abstract "Levoglucosenone (1) is produced in ca. 12% yield from cellulose. The preparation is carried out under reduced pressure and in the presence of soybean oil and 2.5% phosphoric acid based on the cellulose mass. Various factors are investigated to determine the effect they have on the yield of 1 from cellulose, and the optimized procedure is given. Levoglucosenone (1) can be made on the gram scale using this process, and the vacuum distillation of the compound results in a purity of greater than 90%. This procedure is the most convenient way to make levoglucosenone on the bench top given to date." @default.
- W44473336 created "2016-06-24" @default.
- W44473336 creator A5086270282 @default.
- W44473336 date "2018-08-13" @default.
- W44473336 modified "2023-09-27" @default.
- W44473336 title "An improved preparation of levoglucosenone from cellulose" @default.
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- W44473336 doi "https://doi.org/10.31274/rtd-180813-16564" @default.
- W44473336 hasPublicationYear "2018" @default.
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