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• W50210917 abstract "A sol–gel reaction starting from Si and Zr alkoxides, in water–ethanol mixtures, was employed to obtain praseodymium doped zirconium silicate powders (zircon). The reactions were performed by modulating both: (a) the amount of praseodymium salt in the starting mixture and (b) the speciation of the mineralizers; chloride and fluoride salts of monovalent (Na+, Li+) and divalent (Mg2+) were tested. The products of the sol–gel reaction were calcined either at 1000 °C or at 1200 °C. The samples were characterised by X-ray diffraction, SEM micrographs, EDX analyses and diffuse reflectance spectroscopy; the colour of the pigments was characterized on the grounds of the Commission Internationale de l’Eclairage (CIE) standard procedure (CIE L∗a∗b∗ measurements). Results from the structural, morphological and optical characterisations are examined and cross-compared to produce a consistent picture of the key factors leading to the formation, growth and optical properties of the reaction products." @default.
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• W50210917 date "2004-11-01" @default.
• W50210917 modified "2023-10-14" @default.
• W50210917 title "Yellow Pr-zircon pigments" @default.
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• W50210917 doi "https://doi.org/10.1016/j.jeurceramsoc.2004.01.003" @default.
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