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• W5383251 abstract "A hybrid nanocomposite formed by interaction of a octa (3-chloropropyl)octasilsesquioxane modified with imidazol and its subsequent reaction with cadmium and hexacyanoferrate (II) (CdHSSI) was incorporated into a graphite paste electrode and the electrochemical studies were conducted with cyclic voltammetry. The cyclic voltammogram of the modified graphite paste electrode with CdHSSI (GPE- CdHSSI), showed one redox couple with formal potential E?=0.14V (vs Ag/AgCl, NaNO3, 1.0 mol L-1; v = 20 mV s-1), attributed to the Fe2+(CN)6/ Fe3+(CN)6 process. The redox couple presents an electrocatalytic response for determination of ascorbic acid. The modified electrode gives a linear range from 2.0í10-4 mol L-1 to 9.0í10-4 mol L-1 (r=0.998) for the determination of ascorbic acid with detection limit of 1.21í10-4 mol L-1 with a relative standard deviation of 5% (n=3) and amperometric sensitivity of 6.217 mA/ mol L-1 for ascorbic acid." @default.
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• W5383251 date "2013-01-01" @default.
• W5383251 modified "2023-10-05" @default.
• W5383251 title "Voltammetric Study of a Cubic Silsesquioxane Organically Modified with Imidazole and their Subsequent Reaction with Cadmium and Hexacyanoferrate (III)" @default.
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• W5383251 doi "https://doi.org/10.1016/s1452-3981(23)14064-8" @default.
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