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- W561238018 abstract "A hydrothermal reaction of zinc acetate with molybdenum trioxide, vanadiumpentoxide, phosphorus pentoxide and 2,2′-bpy (2,2′-bipyridine) led to the title compound [Zn(2,2′-bpy)2(HaO)]2[HPMo12O40(VO)2] 1. Single-crystal X-ray diffraction revealed that 1 (C40H36-N8O44PV2Zn2Mo12) crystallizes in the triclinic system, space group P1 with a=11.881(2), b =12.468(2), c=12.622(2)A, α=71.333(8), β=74.485(4), γ=86.896(5)°, V= 1705.8(4)A^3, Mr=2747.64, Z=1, Dc=2.675g/cm^3, μ=3.201mm^-1, F(000)=1309, S=1.070, the final R=0.0697 and wR=0.1905 for 5368 observed reflections with I > 2σ(I). Compound 1 is built on a mixed-metal bicapped [HPMo12V2O42] subunit covalently bonded to two [Zn(2,2′-bpy)2(H2O)]^2+ clusters via terminal oxygen atoms of the capping V atoms. Each Zn atom is six-coordinated by fournitrogen atoms from two 2,2′-bpy ligands, one terminal oxygen atom from coordinated water molecule and another one from the capped {VO} unit." @default.
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- W561238018 date "2005-01-01" @default.
- W561238018 modified "2023-09-23" @default.
- W561238018 title "Hydrothermal Synthesis and Crystal Structure of a Bivanadyl Capped Keggin Polyoxometalate [Zn（2,2′-bpy）2（H2O）]2[HPMo12040（VO）2]" @default.
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