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- W57018284 abstract "Although the vast majority of 15N spectra is now directly recorded by pulse FT spectroscopy, indirect detection may still be of interest. Indeed, a lot of 15N parameters have been obtained in the past through CW double resonance experiments. In this area, the various techniques of 1H{15N}double irradiation can be exploited and information about the 15N resonances is then obtained via proton responses to perturbations applied, more or less selectively, to the 15N transitions (M 31d). The INDOR method, in particular, is well suited to indirect detection of the 15N spectrum (M 28) (M 33). In this method a proton line corresponding to a given 15N~H scalar coupling is continuously monitored while the double irradiation field ( overrightarrow {{B_2}} ) is swept with an amplitude *B2 ≃ ∆υ1/2 (HZ) through the 15N transitions. Responses are then obtained in the 1H spectrum each time that the double irradiation frequency encounters a 15N transition connected with the considered proton line. This technique allows a determination of the 15N coupled spectrum which benefits from the sensitivity of the corresponding proton resonances. However, it requires the existence of detectable 15N~H coupling constants and lacks general applicability." @default.
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- W57018284 date "1981-01-01" @default.
- W57018284 modified "2023-10-02" @default.
- W57018284 title "Experimental Techniques in 15N Spectroscopy" @default.
- W57018284 doi "https://doi.org/10.1007/978-3-642-50172-2_3" @default.
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