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- W570546136 abstract "The subject of this study is the development of a bottom-up method for the preparation of nano-scaled Magneli phases. There are two steps involved; the first step is sol-gel preparation of Ti(OH)4 using titanium tetraisopropoxide as organometallic precursor, and the second step is its thermal decomposition to TiO2 or Magneli phases. Thermal treatment in an oxidative atmosphere (air) was performed at different temperatures to produce TiO2 in order to determine the regions of stability of anatase and rutile. Next, thermal treatment in a reductive (10 % H2 + 90 % N2) atmosphere at temperature of rutile was performed to produce Magneli phases. Furthermore, a top-down approach was applied to produce non-stoichiometric titanium oxides by mechanical activation of commercial Magneli phases known as Ebonex. Examples of the application of top-down produced Magneli phases in electro- and photocatalysis are shown." @default.
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- W570546136 date "2014-12-19" @default.
- W570546136 modified "2023-09-26" @default.
- W570546136 title "Pathways for the Production of Non-stoichiometric Titanium Oxides" @default.
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- W570546136 doi "https://doi.org/10.1007/978-94-017-9697-2_24" @default.
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