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- W57721820 abstract "A direct power measuring Differential Scanning Calorimeter, such as the Perkin-Elmer DSC-1B, has both unique capabilities and unique design problems. The juxtaposition of heating and sensing elements in a low thermal mass sample holder puts particular strain on the temperature programmer. Programming noise and fluctuations are not thermally filtered or smoothed by large furnace systems as in conventional designs. Also, for rapid programmed cooling experiments and quick turn-around times, it is desirable that the immediate environment of the sample holders be maintained at low temperature. Consequently, large temperature gradients can exist between sample holders and surroundings which can affect baseline reproducibility and linearity. Further, the benefits of direct power measurement are realizable only through a considerably more complex sample holder construction than typical of AT measuring systems. This has limited the extension of DSC to higher temperatures. In this paper these problems will be discussed, solutions proposed, and the performance of an experimental extended range DSC incorporating some new design features will be briefly described." @default.
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- W57721820 date "1972-01-01" @default.
- W57721820 modified "2023-09-24" @default.
- W57721820 title "Design Considerations in Advanced Systems for Differential Scanning Calorimetry" @default.
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- W57721820 doi "https://doi.org/10.1007/978-3-0348-7413-7_24" @default.
- W57721820 hasPublicationYear "1972" @default.
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