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• W577692919 endingPage "7567" @default.
• W577692919 startingPage "7564" @default.
• W577692919 abstract "A new strategy is reported for intramolecular sp(3) C-H amination under mild reaction conditions using iodoarene as catalyst and m-CPBA as oxidant. This C-H functionalization involving iodine(III) reagents generated in situ occurs readily at sterically hindered tertiary C-H bonds. DFT (M06-2X) calculations show that the preferred pathway involves an iodonium cation intermediate and proceeds via an energetically concerted transition state, through hydride transfer followed by the spontaneous C-N bond formation. This leads to the experimentally observed amination at a chiral center without loss of stereochemical information." @default.
• W577692919 created "2016-06-24" @default.
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• W577692919 date "2015-06-11" @default.
• W577692919 modified "2023-10-17" @default.
• W577692919 title "Iodoarene-Catalyzed Stereospecific Intramolecular sp³ C–H Amination: Reaction Development and Mechanistic Insights" @default.
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• W577692919 doi "https://doi.org/10.1021/jacs.5b03488" @default.
• W577692919 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/26035639" @default.
• W577692919 hasPublicationYear "2015" @default.
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