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- W5837390 abstract "Abstract Silicalite samples containing tetravalent metals (Ge, Ti, Zr) have been hydrothermally synthesized and characterized by various spectroscopic and thermoanalytic methods. Zr-Sil. shows nearly no increase of the unit cell volume. Strong indications for an incorporation of Zr in the framework arise from a Raman band at 685 cm- 1 and a DTA peak that is about 30 K higher than for silicalite. In contrast to silicalite a symmetry change from orthorhombic to monoclinic is not observed. In Ge-Sil. a 29 Si NMR signal at -110 ppm of Si-O-Ge groups can be resolved under optimal conditions only. Combined Raman (band at 960 cm −1 ), XPS and ESR measurements of Ti-Sil. allow to distinguish between Ti isomorphously substituting Si in the framework and between extra-framework Ti" @default.
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- W5837390 date "1994-01-01" @default.
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- W5837390 title "Study on the Isomorphous Substitution of Silicon by Tetravalent Elements (Zr, Ge, Ti) in the Framework of MFI Type Zeolites" @default.
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- W5837390 doi "https://doi.org/10.1016/s0167-2991(08)63242-5" @default.
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