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- W58957029 abstract "Here we report the synthesis of several aluminophosphates including the polymeric [AlP 2 O 8 H 2 ] − [Et 3 NH] + , the 20-membered ring JDF-20 framework, the porous macroanionic [Al 3 P 4 O 16 ] 3- AlPO 4- 5-like sheet structure, AlPO 4- 5, tinsleyite and AlPO 4 -cristobalite, all from a tetraethylene glycol - water solvent system and a 2:1 P:Al gel. The cocrystallization as well as the structural similarities between the [AlP 2 O 8 H 2 ] − [Et 3 NH] + chain and the JDF-20 phase together provide new insight into the mode of formation of aluminophosphate molecular sieves and allows one to postulate reaction pathways for the transformation between the two phases. The water content of the reaction mixture appears to play a crucial role in determining the nature of the final products. The hydrolysis of polymeric [AlP 2 O 8 H 2 ] − to various related chain structures followed by their ordered condensation, permits the formation of the “building blocks” of a wide range of AlPO 4 -n structures, such as VPI-5, AlPO 4- 5, AlPO 4- 11, tinsleyite and many others, as well as dense aluminophosphate phases, such as, AlPO 4 -cristobalite." @default.
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- W58957029 date "1994-01-01" @default.
- W58957029 modified "2023-10-16" @default.
- W58957029 title "New Insights into the Mode of Formation of AIPO4-n Molecular Sieves" @default.
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- W58957029 doi "https://doi.org/10.1016/s0167-2991(08)64117-8" @default.
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