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• W592076266 abstract "At present work, a ZrB2–SiC/SiC gradient coating has been fabricated via in-situ reaction in one-step of heat-treatment. Si–ZrB2 composite coating was previously prepared on C/C composites using vacuum plasma spray (VPS) technology and then ZrB2–SiC/SiC gradient coating was synthesized by heat-treatment. In order to investigate the formation mechanism of the gradient coating, the as-sprayed Si–ZrB2 samples were heat-treated at varied temperatures from 1300 °C to 2000 °C. The ablation resistance of the gradient coating was explored by comparison test with monolayer SiC coating using H2–O2 flame. Results showed that most of the ZrB2 particulates were detained in near-surface of coating while liquid Si infiltrated into the C/C substrate during the heat-treatment. A ZrB2–SiC/SiC gradient coating could be synthesized when the heating temperature was suitable (such as 1800 °C) to obtain a moderate viscosity for liquid Si, which allowed the concurrence of ZrB2 particulates' transportation and the infiltration and reaction of Si within carbon substrate. Better ablation resistance was confirmed for the ZrB2–SiC/SiC gradient coating by the ablation tests as compared with simple SiC coating. The gradient coating could withstand the H2–O2 flame (above 2500 °C, atmosphere) for at least 300 s." @default.
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• W592076266 date "2015-10-01" @default.
• W592076266 modified "2023-10-16" @default.
• W592076266 title "In-situ fabrication of ZrB2–SiC/SiC gradient coating on C/C composites" @default.
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• W592076266 doi "https://doi.org/10.1016/j.jallcom.2015.05.205" @default.
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