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- W598328938 abstract "以腺嘌呤（1）为原料,经过氧化、水解、还原、环合和与S-烷基化反应得到2-烷硫基腺嘌呤（6）;甲烷三羧酸三乙酯与1,2-二溴乙烷反应得到3-溴丙烷-1,1,1-三羧酸三乙酯（7）;6和7在碱性条件下反应得到3-（6-氨基-2-烷硫基-9H-嘌呤-9-基）丙烷-1,1,1-三羧酸三乙酯（8）;8在甲醇钠作用下发生脱酯基和酯交换反应,得到目标化合物2-（2-（6-氨基-2-烷硫基-9H-嘌呤-9-基）乙基）丙二酸二甲酯（9）。通过FT-IR、1H-NMR、13C-NMR及HRMS对6种新的无环嘌呤核苷化合物8和9的结构进行了确证。" @default.
- W598328938 created "2016-06-24" @default.
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- W598328938 date "2011-11-20" @default.
- W598328938 modified "2023-09-23" @default.
- W598328938 title "无环嘌呤核苷化合物2-(2-(6-氨基-2-烷硫基-9H-嘌呤-9-基)乙基)丙二酸二甲酯的合成" @default.
- W598328938 hasPublicationYear "2011" @default.
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