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• W613157923 abstract "The origin of gas-liquid partition chromatography is generally taken to be a 1941 comment by A. J. P. Martin indicating that it should be possible to use a gas and a liquid in a partition Chromatographic separation (Martin and Synge, 1941). In 1948–1949 experimental work was undertaken, and the results of the first successful experiments were published in 1952 (James and Martin, 1952). The separation of fatty acids was studied, and the theoretical basis of GLC separations was discussed. The separation of organic amines was investigated in later work. The need for gas phase detection systems became evident as soon as compounds other than acids and bases were studied. The separation of hydrocarbons, for example, was (and is) an application of great importance to the petroleum industry, but this separation problem could not be studied effectively without suitable detectors. During the next few years many types of detection systems were developed. The “gas density balance” of Martin and James (1956) had moderately high sensitivity. The response was on a molar basis, and this detector was used extensively at Mill Hill (National Institute for Medical Research, London). Thermal conductivity detection systems (Claesson, 1946; Ray, 1954) came into wide use in studies where the sample was relatively large, while the argon ionisation detector with a radium foil source was used as a sensitive detection system with microgram samples (Lovelock, 1958). The hydrogen flame ionization detection system was developed through work in several laboratories around 1957–1958, and this detector is now used universally in quantitative work with samples down to about 0.01 μg." @default.
• W613157923 created "2016-06-24" @default.
• W613157923 creator A5027942054 @default.
• W613157923 date "1968-01-01" @default.
• W613157923 modified "2023-10-15" @default.
• W613157923 title "Gas Phase Analytical Methods for the Study of Steroid Hormones and their Metabolites" @default.
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• W613157923 doi "https://doi.org/10.1007/978-3-662-35229-8_1" @default.
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