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- W61392565 abstract "Our data indicate that evaporation is the rate-limiting step in film formation when the temperature of a latex is about 20 K or more above its glass transition temperature (Tg). When a latex is nearer to its Tg, the rate-limiting step in film formation is deformation of the latex particles, possibly by viscous flow of the polymer driven by the reduction in surface energy. In this latter case, there is evidence that a drying front first creates air voids. Subsequently, a coalescence front moves inward from the periphery in the plane of the film. Evaporation rates are retarded in a latex that is well-above its Tg, probably as a result of the reduced surface area of water, caused by extensive particle deformation. We studied the kinetics of film formation in an acrylic latex using ellipsometry and environmental-SEM, techniques which allow in situ observation of wet and partially-wet latices. We fit our data to a model describing the coalescence of voids by viscous flow." @default.
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- W61392565 date "1996-10-15" @default.
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- W61392565 title "Rate-Limiting Steps in Film Formation of Acrylic Latices as Elucidated with Ellipsometry and Environmental Scanning Electron Microscopy" @default.
- W61392565 doi "https://doi.org/10.1021/bk-1996-0648.ch021" @default.
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