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- W61578777 abstract "In this paper, we investigate the deposition of Sb and Sb-Bi nanocrystalline films from the chloride, citrate, and tartrate electrolytes. It is found that the most suitable electrolyte for glossy films of perfect quality is the alkaline tartrate electrolyte (0.25 mol/dm 3 KNaC 4H 4O 6, 0.2 mol/dm 3 KOH, 0.01 mol/dm 3 SbCl 3 and 0.01 mol/dm 3 bismuth tartrate) with PA-1 as an additive. It is possible to use the alkaline citrate electrolyte. It is necessary to apply low current density, not more than 0.4 A/dm 2, to obtain glossy films. It is important to treat the base surface on which the metal or alloy film is deposited. It is impossible to obtain nanoparticles and nanocrystalline structure on the poorly polished surface. Obviously, if the microcrystal size is smaller than the short light wave length, the microroughness on the surface is invisible and the residue has a full gloss. With the atomic force microscope used, the investigation of Sb and Sb-Bi samples confirms that the film nanocrystalline structure is formed. The films of perfect quality are formed at any ratio of concentrations of antimony (III) and bismuth (III) in the solution. Sb-Bi electroplating can be used for further study of their electrical and mechanical properties." @default.
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- W61578777 date "2013-01-01" @default.
- W61578777 modified "2023-09-23" @default.
- W61578777 title "Электрохимическое осаждение нанокристаллических пленок Sb и Sb-Bi" @default.
- W61578777 hasPublicationYear "2013" @default.
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