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- W625176088 abstract "Fusion reaction of methyl salicylate and secondary amines afforded salicylamide compounds in a low yield only in the case of 1, 2, 3, 4-tetrahydroisoquinoline (I) and piperidine, and the amide compound was not obtained in the case of 1, 2, 3, 4-tetrahydroquinoline (II), N-methylbenzylamine (III), N-methylaniline (IV), and diphenylamine (V), forming N-methylated tertiary amines as the main product. Further, when such tertiary amines were 2-methyl-1, 2, 3, 4-tetrahydroisoquinoline (VII) and N, N-dimethylbenzylamine, quaternary ammonium salicylate was also formed. When the secondary amine was a comparatively strong base like I, salicylate of I was also found to be formed as a by-product." @default.
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- W625176088 date "1967-01-01" @default.
- W625176088 modified "2023-10-14" @default.
- W625176088 title "A Novel Alkylation. IV : N-Alkylation of Secondary Amines with Methyl Salicylate : Studies on the Syntheses of Heterocyclic Compounds. CLXXI" @default.
- W625176088 doi "https://doi.org/10.1248/yakushi1947.87.3_265" @default.
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