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- W6260902 abstract "This chapter describes the kinetics of the early stage of dispersion polymerization in supercritical CO 2 . The early stage of dispersion polymerization of MMA in SC-CO 2 has been studied by turbidimetry. The average number of particles, the turbidity-average diameter, and the mass of polymer as a function of time has been derived from these data for conversions lower than 0.1%. In the early stages investigated here, the polymerization solely takes place in the homogeneous phase. This can be concluded from the kinetic analysis of the reaction rates and from a comparison of the experimental rates with theoretical estimates. The dispersion polymerization proceeds through two stages. In stage I, the polymer forms new particles with a critical diameter of 150–170 nm. After this very short period of particle formation, all polymers precipitate on the particles. The rate of polymerization, however, remains constant in all stages. The experimental data derived from this analysis are in semiquantitative agreement with the model proposed by Paine." @default.
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- W6260902 date "2004-01-01" @default.
- W6260902 modified "2023-09-26" @default.
- W6260902 title "The kinetics of the early stage of dispersion polymerization in supercritical CO 2" @default.
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- W6260902 doi "https://doi.org/10.1016/b978-044451574-2/50023-7" @default.
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