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- W644423412 abstract "Chemoselective addition of (difluoromethyl)trimethylsilane (CHF2SiMe3) to the carbonyl bond of aryl glyoxal derived α-imino ketones, and selected diaryl 1,2-diketones were studied in the presence of initiators, such as potassium tert-butoxide or caesium fluoride. Subsequent reduction of the obtained α-imino alcohols and α-hydroxy ketones with sodium borohydride gave the expected 2-amino 1-(difluoromethyl)alcohols and (difluoromethyl)-1,2-diols respectively in moderate to good yields. High de values were observed for the reduction of α-(difluoromethyl)-α-hydroxy ketones." @default.
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- W644423412 date "2015-08-01" @default.
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- W644423412 title "Nucleophilic addition of (difluoromethyl)trimethylsilane to selected α-imino ketones and aryl diketones" @default.
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- W644423412 doi "https://doi.org/10.1016/j.tetlet.2015.06.025" @default.
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