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• W647184089 abstract "We apply chirality sensitive microwave three-wave mixing to 4-carvomenthenol, a molecule previously uncharacterized with rotational spectroscopy. We measure its rotational spectrum in the 2-8.5 GHz range and observe three molecular conformers. We describe our method in detail, from the initial step of spectral acquisition and assignment to the final step of determining absolute configuration and enantiomeric excess. Combining fitted rotational constants with dipole moment components derived from quantum chemical calculations, we identify candidate three-wave mixing cycles which were further tested using a double resonance method. Initial optimization of the three-wave mixing signal is done by varying the duration of the second excitation pulse. With known transition dipole matrix elements, absolute configuration can be directly determined from a single measurement." @default.
• W647184089 created "2016-06-24" @default.
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• W647184089 date "2015-06-02" @default.
• W647184089 modified "2023-10-16" @default.
• W647184089 title "Rotational spectroscopy and three-wave mixing of 4-carvomenthenol: A technical guide to measuring chirality in the microwave regime" @default.
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• W647184089 doi "https://doi.org/10.1063/1.4921833" @default.
• W647184089 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/26049489" @default.
• W647184089 hasPublicationYear "2015" @default.
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