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- W66749244 abstract "Publisher Summary This chapter discusses the conformational analysis via nuclear magnetic resonance (NMR) spectroscopy. The NMR method—as applied to conformationally mobile carbohydrate derivatives—has successfully demonstrated that electric dipole–dipole interactions are frequently more important than steric interactions in determining the relative stabilities of conformations. A further advantage of the NMR technique is that, in simple cases, mere inspection of the NMR spectrum of a compound may suffice to identify its favored conformation. Considerable computation is necessary for the diffraction methods, but the resulting conformation is determined very precisely and in great detail. It should not be assumed that this conformation necessarily resembles closely that favored in solution because the forces in the two environments are different. Because of the low sensitivity of the NMR method, it is usually advisable to use as high a solution concentration as possible. The choice of the NMR method to be used for conformational analysis is very dependent on the exact structure of the molecule to be examined and on whether multiple bonds or magnetic nuclei other than protons are present." @default.
- W66749244 created "2016-06-24" @default.
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- W66749244 date "1972-01-01" @default.
- W66749244 modified "2023-10-17" @default.
- W66749244 title "Conformational Analysis via Nuclear Magnetic Resonance Spectroscopy" @default.
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- W66749244 doi "https://doi.org/10.1016/b978-0-12-746206-6.50100-4" @default.
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