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- W6934129 abstract "A new fluorinated microporous gallophosphate ULM-5 or Ga16(PO4)14(HPO4)2(OH)2F7. 4 H3N(CH2)6NH3. 6 H2O, was obtained by hydrothermal synthesis(453 K, 24 h, autogeneous pressure) from a mixture of Ga2O3, P2O5, HF, 1,6-diaminohexane and H2O in the ratio 1:1:2:1:80. It is orthorhombic(space group: P22121(n°18)) with a = 10.252(2) Å, b = 18.409(4) Å, c = 24.639(7) Å, V = 4649.8(9) Å3, Z = 2. The three-dimensional network is built up from three types of basic building units: two are hexameric in which the fluorine atoms are bridging two gallium atoms; the third is octameric(D4R) with encapsulated fluorine atom. The framework delimits 16- and 6-membered ring channels along [100] and 8-membered ones along [010]. The diprotonated amines are inserted in the 16-membered ovoid channels, whose free aperture is 12.2 × 8.3 Å. The water molecules are in the 6-membered tunnels. The NMR study was undertaken using the different observable nuclei 71Ga, 31P, 19F, 15N, 13C and 1H." @default.
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- W6934129 date "1994-01-01" @default.
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- W6934129 title "Synthesis and characterization by X-ray diffraction and solid state NMR of ULM-5, a new fluorinated gallophosphate Ga16(P04)14(HP04)2(OH)2F7. 4 H3N(CH2)6NH3. 6 H20 with 16-membered rings." @default.
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- W6934129 doi "https://doi.org/10.1016/s0167-2991(08)64138-5" @default.
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