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• W72888830 abstract "Studies performed over multi-phase selective oxidation catalysts such as MnMoO4/MoO3 and CdMoO4/MoO3 for the partial oxidation of C4 hydrocarbons have shown the presence of strong synergy effects. This phenomenon was investigated through detailed catalyst characterization and reaction kinetics studies. Pure phases as well as multi-phase catalysts were characterized using techniques such as BET surface area, X-ray diffraction, scanning electron microscopy, energy dispersive X-ray analysis, laser Raman spectroscopy and X-ray photoelectron spectroscopy. Steady-state reaction experiments examining the effect of oxygen partial pressure, transient response studies using isotopic labeling, and oxygen chemisorption experiments were performed to investigate the catalytic job distribution among different components of the active catalyst. More recent studies combining in-situ laser Raman spectroscopy with isotopic labeling technique provided further evidence of the mechanism of synergy in these model multi-phase catalysts. Using a specially designed in-situ cell, samples were reduced by 1,3-butadiene and then reoxidized by labeled oxygen, thus allowing observation of Raman band shifts which could be identified with catalytic sites responsible for specific steps in the oxidation scheme." @default.
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• W72888830 date "1992-01-01" @default.
• W72888830 modified "2023-09-27" @default.
• W72888830 title "Synergy Effects in Selective Oxidation Catalysis" @default.
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• W72888830 doi "https://doi.org/10.1016/s0167-2991(08)61686-9" @default.
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