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- W76807938 abstract "Abstract A simple, accurate, and effective capillary electrophoresis method with ultraviolet absorbance detection was developed and validated for the quantitation of the antihistamine fexofenadine in capsules. The separation was performed with an uncoated fused-silica capillary (47 cm × 75 μm id) and was operated at 20 kV potential. Temperature was maintained at 25°C. The run buffer was prepared with 20mM Na2B4O7 × 10 H2O. Software was used for system control, data acquisition, and analysis. Method validation was performed by evaluation of the analytical parameters linearity, precision, accuracy, limits of detection and quantitation, and specificity. The method was linear (r = 0.9999) at concentrations ranging from 20 to 100 μg/mL, precise (relative standard deviation intra-assay = 1.2, 1.6, and 1.8% and interassay = 1.5%); accurate (recovery = 98.1%); and specific. The limits of detection and quantitation were 0.69 and 2.09 μg/mL, respectively. The method was compared to the liquid chromatography method developed previously by the authors for the same drug, and no significant difference was found between the 2 methods in fexofenadine hydrochloride quantitation." @default.
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- W76807938 date "2005-07-01" @default.
- W76807938 modified "2023-09-25" @default.
- W76807938 title "Capillary Electrophoresis Method for Fexofenadine Hydrochloride in Capsules" @default.
- W76807938 doi "https://doi.org/10.1093/jaoac/88.4.1059" @default.
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