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- W77772765 abstract "Addition of the elements of phthalimide to methyl 2,3-anhydro-4,6-O-benzylidene-α-d-mannopyranoside (1) under fusion conditions has yielded methyl 4,6-O-benzylidene-3-deoxy-3-phthalimido-α-d-altropyranoside (2). The conformation of the pyranose ring of 2 has been shown to be non-chair by 1H NMR spectroscopy, in contrast to the conformations of related derivatives having smaller substituents at C-3. Molecular dynamics simulations of 2 in explicit chloroform-d solvent have indicated four principal conformational possibilities. Of these, the 7C5/1S5 chair/skew boat form 2d has the lowest potential energy, and is largely consistent with the observed vicinal 1H–1H NMR coupling constants." @default.
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- W77772765 date "2001-04-01" @default.
- W77772765 modified "2023-09-26" @default.
- W77772765 title "Boat conformations" @default.
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- W77772765 doi "https://doi.org/10.1016/s0008-6215(01)00036-2" @default.
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