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- W788100729 abstract "With a view to understanding the argument of the phase transition mechanisms of D- and L- valine around 270 K, the temperature dependences of the heat capacities of single crystals, ground powders, and polycrystalline products were investigated using differential scanning calorimetry. Endothermic transition peaks were observed at phase transition temperatures of 273.59 and 273.76 K for D- and L-valine single crystals, respectively with an energy difference of 0.18 J∙mol - 1 . The X-ray crystal fine structure of chiral valine was determined using Mo-Kα radiation (λ=0.071073 nm) on Nonius Kappa CCD diffractometer. D- and L-valine crystals were monoclinic, with the P21 space group, Z=4, lattice constants a= 0.96706(5)/0.96737(5) nm, b=0.52680(3)/0.52664(3) nm, and c=1.20256(7)/1.20196 (6) nm, and β=90.724(2)°/ 90.722(3)° at ~270 K. Two crystallographically independent molecules A (trans form) and B (gauche I from)" @default.
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- W788100729 date "2014-01-01" @default.
- W788100729 modified "2023-10-16" @default.
- W788100729 title "Crystal Fine Structure and Optical Rotatory Angle Study on Spin Superfluidity of Intermolecular N<sup>+</sup>H…O<sup>- </sup>Hydrogen Bond Electron Cooper Pairing onto D-, L-, and DL-Valine Optical Lattices" @default.
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- W788100729 doi "https://doi.org/10.3866/pku.whxb201402181" @default.
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