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- W802277436 abstract "[(tacn) 4 Fe 4 O 2 (OH) 4 ] 2 .8Br.9H 2 O (tacn = 1,4,7-triazacyclononane), a tetranuclear iron(III) complex was synthesized by the hydrolysis of (tacn)FeCl 3 and crystallizes in the orthorhombic space group, Pca2(1), with cellparameters, a = 37.574(3) A, b = 16.9245(12) A, c = 14.2830(11) A, V = 9082.9(12) A 3 . [(tacn) 4 Fe 4 O 2 (OH) 4 ] 4 + cations approach S 4 point symmetry containing an adamantane skeleton. Four Fe(III) atoms have distorted octahedral environments with two hydroxo and an oxo bridges. Two [(tacn) 4 Fe 4 O 2 (OH) 4 ] 4 + clusters having different Fe...Fe distances are connected to each other by the networked hydrogen bonds. The electrochemical behavior reveals irreversible three cathodic and two anodic peaks. Magnetic properties are characterized by antiferromagnetic (AF) interactions between Fe(III) ion spins. However, the low-lying states are still magnetic and exhibit a blocking behavior and a magnetic hysteresis at low temperatures." @default.
- W802277436 created "2016-06-24" @default.
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- W802277436 date "2005-02-20" @default.
- W802277436 modified "2023-09-25" @default.
- W802277436 title "Crystal Packing of Two Different Tetranuclear Iron(III) Clusters, [(tacn)4Fe4O2(OH)4]2.8Br.9H2O (tacn = 1,4,7-triazacyclononane)" @default.
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- W802277436 doi "https://doi.org/10.5012/bkcs.2005.26.2.253" @default.
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