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- W804913452 abstract "A method of reversed phase high performance liquid chromatography (HPLC) with internal standard was applied to the quantitative analysis of 1, 15-pentadecanedioic acid, which was an important material in the synthesis of cyclopentadecanolide. Optimum conditions were determined as follows: column packed with C18 (4.6×250 mm), lauric acid as internal standard. The mobile phase consists of a mixture of methanol, acetonitrile and water (80:5:15, 0.1% trifluoroacetic acid) with a flow rate of 1.2 mL/min and UV detection performed at 210nm. Desired relativity (γ＞0.9990) and analytic precision (RSD＜1%) were obtained by the method with average recovery rate of 99.25% and sensitivity of 4.543×10^(-4)g/(s•L)." @default.
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- W804913452 date "2010-10-30" @default.
- W804913452 modified "2023-09-23" @default.
- W804913452 title "高效液相色谱法测定1,15-十五碳二元酸的方法研究" @default.
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