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- W809325145 abstract "SYNOPSIS. The information of saccharides qualitative presence and quantitative abundance in lignocellulosics is very important from the viewpoint of the saccharides structure knowledge. In the paper the optimization is described of sugar aldonitrilacetates capillary gas chromatography method and its evaluation for the separation and quantification of carbohydrates in various samples. For the monosaccharides identification six aldonitrilacetates of standard carbohydrates (rhamnose, arabinose, xylose, manose, glucose, galactose) were prepared. Three sulphate spruce pulps were hydrolysed by Saeman et al. (1954) method. Also holocellulose was prepared by Wise et al. (1946) method from beech wood before and after prehydrolysis. Then the samples were derivatised to aldonitrilacetates. The gas chromatography was performed on Fisons 8310 DPFC GC with flame ionisation detector and DB-5 capillary column with inositol as an internal standard. The retention times, response factors, resolution and recovery of the standard carbohydrates aldonitrilacetates were received. The obtained results of the saccharides determination in the pulps and holocellulose showed the suitability of aldonitrilacetates for the saccharides from cellulosics analysis by method of the capillary gas chromatography." @default.
- W809325145 created "2016-06-24" @default.
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- W809325145 date "2009-01-01" @default.
- W809325145 modified "2023-09-23" @default.
- W809325145 title "Determination of carbohydrates in lignocellulosics by gas chromatography of aldonitrilacetates" @default.
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