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- W816028297 abstract "The structures of (x = 4.3 and 3.25), vacuum dehydrated zeolite A with all ions replaced by and as indicated, have been determined by single-crystal X-ray diffraction techniques in cubic space group Pm3m at 21(1) (a=12.100(2) for and a=12.092(2) for ). The crystals of and were prepared by flow method using exchange solutions in which mole ratios of $TlNO_3$,/TEX> and were 1:50 and 1:1, respectively, with total concentration of 0.05 M. The structures of the dehydrated and were refined to yield the final error indices = 0.075 and = 0.075 with 236 reflections, and = 0.057 and = 0.064 with 202 reflections, respectively, for which I > 3(I). Both structures indicate that Zn(II) ions are coordinated by three framework oxygens: the Zn(II) to O(3) distances are 2.08(1) for and 2.07(1) for , respectively. In each structure, the angle subtended at Zn(II), O(3)-Zn(II)-O(3) is 119.9(3) for , and 120.0(3) for , respectively, close to the idealized trigonal-planar value. Zn(II) ions prefer to 6-ring sites. ions do not have any preference to a particular site but occupy simultaneously both at the 6-ring sites and 8-ring sites." @default.
- W816028297 created "2016-06-24" @default.
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- W816028297 date "1990-01-01" @default.
- W816028297 modified "2023-09-24" @default.
- W816028297 title "Two Crystal Structures of $Tl^+$ and $Zn^{2+}$ Exchanged Zeolite A, $Tl_{12-2x}Zn_x-A$ (x=4.3 and 3.25)" @default.
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