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- W8172847 abstract "Crystal structure of the title compound C16H25O2NS2 has beendetermined by X-ray diffraction method. Its crystallographic data were as follows: Mr=327.51, triclinic, space group P1, a=8.864(3), b=10.127(4), c=10.390(3) A, α=105.94(3), β=103.10(2), γ=90.96(3)°, V=870.3(7)A3, Z=2, Dc=1.250g.cm-3, μ(MoKα)=2.966cm-1, F(000)=176, a total of 3275 reflections measured (2θmax=50°), 2246[I≥5σ(I)] used in the refinement, R=0.067, Rw=0.082. The result shows that the distances of N(1)-C(2) and N(1)-C(3) are longer than that of N(1)-C(11), which indicates that the interaction of CAr-Nsp2 is stronger than that of Csp3-Nsp2. Oxygen, nitrogen and sulfur atoms of the ring in the same plane was deduced from the least-squares planes and the dihedral angles." @default.
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- W8172847 date "2001-01-01" @default.
- W8172847 modified "2023-09-28" @default.
- W8172847 title "Synthesis and Crystal Structure of 13—Phenyl—1,10—dithia—4,7—dioxa—13—aza—15—Crown—5" @default.
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