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- W82094841 abstract "Abstract The reaction of pentaphosphaferrocenes [Cp R Fe(η 5 -P 5 )] (Cp R = Cp ∗ = η 5 -C 5 Me 5 , Cp BIG = η 5 -C 5 (4- n BuC 6 H 4 )) with monocationic salts of copper and silver leads to the formation of [{Cp ∗ Fe(η 5 -P 5 )}{Cu(GaCl 4 )} 2 ] n ( 2 ) and [{Cp BIG Fe(η 5 -P 5 )}Ag] n [Al{OC(CF 3 ) 3 } 4 ] n ( 3 ), respectively, representing the rare structural motifs of a 1,2,3,4- or a 1,3-coordination mode of the cyclo -P 5 unit. Both the 2D network as well as the 1D polymer are obtained from self-assembly processes and characterized by X-ray structure analysis. Compound 2 exemplifies a sheet-like structure, whose layers are linked by short Cl⋯H-contacts, whereas the structure of 3 is comprised of cationic strands, whose positive charge is balanced by the weakly coordinating anion [Al{OC(CF 3 ) 3 } 4 ]. Dissociative properties of both polymeric complexes are compared by solution and solid state NMR spectroscopy." @default.
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- W82094841 date "2014-10-01" @default.
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- W82094841 title "Novel polymeric aggregates of pentaphosphaferrocenes and monocationic coinage metal salts – Synthesis of [{Cp ∗ Fe(η 5 -P 5 )}{Cu(GaCl 4 )} 2 ] n and [{Cp BIG Fe(η 5 -P 5 )}Ag] n [Al(OC(CF 3 ) 3 ) 4 ] n" @default.
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- W82094841 doi "https://doi.org/10.1016/j.ica.2014.05.044" @default.
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