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• W821405002 startingPage "6694" @default.
• W821405002 abstract "A synthesis of the fully protected C-ring fragment of the tricyclic diterpene fusicoccin A is reported. The desired cyclopentenyl halides 5a,b are obtained in a total of nine steps. Key transformations of the synthesis sequence are a nonconventional Cr-catalyzed allylic oxidation of a protected intermediate cylcopentenone, a diastereoselective addition of a propenyl Grignard/CeCl3 reagent to the unmasked cyclopentenone, and an asymmetric hydroboration of the isopropenyl substituent. The protected and suitably functionalized C-ring fragment paves the way to explore further the total synthesis of fusicoccin A." @default.
• W821405002 created "2016-06-24" @default.
• W821405002 creator A5048674803 @default.
• W821405002 creator A5062825286 @default.
• W821405002 creator A5090431000 @default.
• W821405002 date "2011-07-28" @default.
• W821405002 modified "2023-09-25" @default.
• W821405002 title "Enantioselective Synthesis of the C₁₀–C₂₀ Fragment of Fusicoccin A" @default.
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• W821405002 doi "https://doi.org/10.1021/jo201020v" @default.
• W821405002 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/21755994" @default.
• W821405002 hasPublicationYear "2011" @default.
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