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- W8439483 abstract "The different stages of SAPO-37 crystallization have been characterized by NMR of 129Xe adsorbed on a series of intermediate phases isolated during synthesis. The nucleation of SAPO-37 occurs within the amorphous phase; the gel then undergoes a preliminary structuration through the formation of large cavities during the aging period. Upon heating at 200°C, the gel transforms into well-defined crystals of SAPO-37. The crystallinity increases with the synthesis time and reaches a maximum after 32h. For longer synthesis times, a crystalline side-phase, SAPO-40, develops in the liquid phase. SAPO-40 has a narrower pore structure than SAPO-37, possibly limited by 12 T puckered rings." @default.
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- W8439483 date "1991-01-01" @default.
- W8439483 modified "2023-09-25" @default.
- W8439483 title "129Xe-NMR Study of the Crystallization of SAPO-37" @default.
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- W8439483 doi "https://doi.org/10.1016/s0167-2991(08)61879-0" @default.
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