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- W86732084 abstract "A high-pressure fractionation column for separation of HfC14 and ZrC14 was built to evaluate the claims of a 1976 Japanese patent (76 65,093). A 35.5-in by 3/4-in ID stainless steel 316 column packed with Inconel 600 helices was operated at 40 kg/sq cm (39 atm) pressure with reboiler and overhead condenser temperatures of 471 and 455 C, respectively. The total reflux operation produced ZrC14, with 800 mol ppm HfC14 in the reboiler and with 5.2 mol pct HfC14 in the overhead. A 4.7-in height equivalent to a theoretical plate was determined using a variable separation factor. Although column corrosion partially obscured the redistribution tendencies of impurities, uranium clearly stayed in the reboiler. Of the potential construction metals exposed during distillation, Inconel 625 and Hastelloy C-276 showed the least corrosion." @default.
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- W86732084 date "1985-12-26" @default.
- W86732084 modified "2023-09-26" @default.
- W86732084 title "High-pressure distillation of crude ZrCl/sub 4/. Open File report" @default.
- W86732084 hasPublicationYear "1985" @default.
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