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• W873603453 abstract "Abstract MnO 2 was homogenously doped into anodic nanotubular TiO 2 by a potential shock method, in which a high potential was imposed on the anodic nanotubes immediately after anodization process. We found that the potential shock process is inapplicable in a high-conductivity aqueous electrolyte, e.g. a MnO 2 precursor solution (herein, 0.006 M KMnO 4 : 852–933 μS/m). To avoid exceeding the output compliance of the current source, the potential shock voltage was optimized in ethylene glycol for the application of water oxidation. We found an optimal potential shock voltage of 140 V, which led to the doping of 0.7 at. % MnO 2 into the high-aspect-ratio nanotubular TiO 2 within 10 s. The TiO 2 nanotubes doped with MnO 2 were successfully employed as electrodes for the non-noble catalysis of water oxidation. Although the doping concentration of Mn was found to be linearly proportional to the applied potential shock voltages, potential shocks greater than 140 V significantly increased the thickness of the barrier oxide layer, which increased the overpotential in the water oxidation process." @default.
• W873603453 created "2016-06-24" @default.
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• W873603453 date "2016-02-01" @default.
• W873603453 modified "2023-10-16" @default.
• W873603453 title "Doping of anodic nanotubular TiO2 electrodes with MnO2 for use as catalysts in water oxidation" @default.
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• W873603453 doi "https://doi.org/10.1016/j.cattod.2015.06.006" @default.
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