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- W874904211 abstract "Studies on subtle spacer ligand effects of AgCF3SO3 with 3,3'-Py2X (X = O vs S) have been carried out. The reaction of AgCF3SO3 with 3,3'-Py2O and 3,3'-Py2S produces [Ag(CF3SO3)(3,3'-Py2O)] and [Ag(3,3'-Py2S)] (CF3SO3), respectively. Crystallographic characterization of [Ag(CF3SO3)(3,3'-Py2O)] (monoclinic P1, a =8.405(2) <TEX>$AA$</TEX>, b = 10.714(2) <TEX>$AA$</TEX>, c = 18.031(2) <TEX>$AA$</TEX>, <TEX>$alpha=$</TEX> 77.36(2), <TEX>$beta=107.83(2)^{circ}$</TEX>, <TEX>$gamma=$</TEX> 66.92(2), V = 1438.0(5) <TEX>$AA3$</TEX> , Z =2,R = 0.0486) reveals that the skeletal structure is an anion-bridged double-strand. The double-strands are packed like a plywood. The framework of [Ag(3,3'-Py2S)](CF3SO3) (orthorhombic Pcab, a = 17.330(2) <TEX>$AA$</TEX>, b = 8.640(1) <TEX>$AA$</TEX>, c = 19.933(6) <TEX>$AA$</TEX>, V = 2985(1) <TEX>$AA3$</TEX> , Z =8, R = 0.0437) is a sinusoidal single-strand. The formation of each coordination polymer appears to be primarily associated with the donating ability and the confor ma-tional energy barrier of the spacer ligands. Thermal analyses indicate that [Ag(CF3SO3)(3,3'-Py2O)] and [Ag(3,3'-Py2S)](CF3SO3) are stable up to 250 <TEX>$^{circ}C$</TEX> and 210 <TEX>$^{circ}C$</TEX>, respectively. For the anion exchangeability, the nature of the spacer ligand is more significant factor than the distance of silver(Ⅰ)···triflate." @default.
- W874904211 created "2016-06-24" @default.
- W874904211 date "2002-08-20" @default.
- W874904211 modified "2023-09-25" @default.
- W874904211 title "Molecular Strands and Related Properties of Silver(Ⅰ) Triflate with 3,3'-Oxybispyridine vs 3,3'-Thiobispyridine" @default.
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- W874904211 doi "https://doi.org/10.5012/bkcs.2002.23.8.1106" @default.
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