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• W875970886 abstract "The reaction of orotic acid (H2or) with trans-[ReOBr3(PPh3)2] in ethanol produced the triply-bridged dimer (μ-Br)(μ-O)(μ-or)[ReIV2Br(OEt)2(PPh3)2] (1). In 2-propanol as solvent the product (μ-Br)(μ-O)(μ-or)[ReIV2Br2(OPri)(PPh3)2] (2) was isolated. In order to eliminate the oxo group as a bridging ligand, the imido-coordinated [ReV{=NC6H4(2-NH2)}Br3(PPh3)2] was reacted with H2or to give the monomer [Re{NC6H4(NH2)}Br(or)(PPh3)2] (3) as product. To remove PPh3 as possible ligand, the reaction of [ReO2(py)4]Cl with H2or produced [ReO(OEt)(or)(py)2] (4). H2or was also reacted with [Re(CO)5Cl], yielding the product (Ph4P)[Re(CO)3(H2O)(or)] (5). The crystal structures of 1–5 were determined by X-ray single crystal diffraction. In addition, infra-red, 1H NMR, electrochemical and electronic properties are also reported." @default.
• W875970886 created "2016-06-24" @default.
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• W875970886 date "2015-09-01" @default.
• W875970886 modified "2023-09-25" @default.
• W875970886 title "Dimeric rhenium(IV) and monomeric rhenium(I) and (V) complexes of orotic acid" @default.
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• W875970886 doi "https://doi.org/10.1016/j.poly.2015.06.006" @default.
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