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- W886563978 abstract "Two novel one-and two-dimensional network structure bismuth(m) complexes with N,N-di(2-hydroxylethyl)aminodithiocarboxylate, {Bi[S2CN(C2H4OH)2]2[1,10-Phen]2(NO3)}·3H2O (1) and {Bi[S2CN(C2H4OH)2]3}2 (2) were synthesized. Their crystal and molecular structures were determined by X-ray single crystal diffraction analysis. The crystal 1 belongs to monoclinic system with space group C2/c, a=1.6431(7) nm, b=2.4323(10)nm, c=1.2646(5) nm, β=126.237(5)°, Z=4, V=4.076(3)nm^3, Dc=1.757 Mg/m^3,μ=4.598 mm^-1, F(000)=2156, R=0.0211, wR=0.0369. The structure shows a distorted square antiprism configuration with eight-coordination for the central Bi atom. The one-dimensional chain structure was formed by H-bonding interaction between hydroxyl group of N,N-di(2-hydroxylethyl)aminodithiocarboxylate ligands and crystal water. The crystal 2 belongs to monoclinic system with space group P2(1)/c, a=1.1149(4)nm, b=2.1274(8) nm, c= 2.2107(8) nm, β=98.325(8)°,Z=4, V=5.188(3) nm^3, Dc=1.920 Mg/m^3,μ=7.315mm^-1 F(000)=2944, R=0.0565, wR=0.0772. The structure shows a distorted square antiprism configuration with eight-coordination for the central Bi atoms. The two-dimensional network structure was formed by H-bonding interaction between adjacent molecules." @default.
- W886563978 created "2016-06-24" @default.
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- W886563978 date "2004-01-01" @default.
- W886563978 modified "2023-09-23" @default.
- W886563978 title "Bismuth（III） Complexes with N,N-Di（2-hydroxylethyl）aminodithiocarboxylate： Synthesis and Crystal Structure of {Bi[S2CN（C2H4OH）2]2[1,10-Phen]2（NO3）}·3H2O and {Bi[S2CN（C2H4OH）2]3}2" @default.
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