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- W88831774 abstract "Abstract The preparations and crystal structures of [PdCl2(R-ahaz)] (ahaz=3-aminohexahydroazepine) and [PdCl2(R-etahaz)] (etahaz=N-ethyl-3-aminohexahydroazepine) are described. Both complexes crystallise with two independent molecules stacked in “dimeric” pairs with short Pd⋯Pd contacts. In [PdCl2(R-ahaz)] the Pd⋯Pd separation is 3.361(1) A and in [PdCl2(R-etahaz)] it is 3.415(1) A. Hydrogen bonds between the N–H groups of one complex and the chloro ligands of the other link the dimers. There are also Pd⋯H contacts in the range 2.60 A to 2.75 A between the ligand backbone and the metal. Molecular mechanics models indicate that the hydrogen bonds are the major contributor to dimer formation." @default.
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- W88831774 date "1999-06-01" @default.
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- W88831774 title "The nature of close Pd⋯Pd and Pd⋯H(—C) contacts" @default.
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- W88831774 doi "https://doi.org/10.1016/s0277-5387(99)00102-3" @default.
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