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- W8895160 abstract "The presence of cyano groups in the stationary phase may provide useful selective interactions during separation. In capillary gas chromatography, the full utility of such interactions will be evident when the columns show high efficiency, good deactivation, high thermal stability and reproducibility in retention characteristics. Columns that fulfil these requirements were prepared. Fused silica capillaries were treated with hydrochloric acid, silanized at a high temperature with cyclic cyanopropylsiloxane and statically coated with cyanopropylsilicone gum, which was finally immobilized by in situ cross-linking. Vulcanization is normally inhibited by cyanopropyl groups, but a certain percentage of tolyl groups in the gum made cross-linking possible. The usefulness of the cyanosilicone columns is demonstrated by the separation of several samples such as fatty acid methyl esters and pheromones." @default.
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- W8895160 date "1983-01-01" @default.
- W8895160 modified "2023-10-16" @default.
- W8895160 title "Cyanosilicones as stationary phases in gas chromatography" @default.
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- W8895160 doi "https://doi.org/10.1016/s0021-9673(01)90816-7" @default.
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