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- W896767401 abstract "This chapter describes the wide range of methods, by which nuclear magnetic resonance (n.m.r) spectroscopy can be used to solve conformational problems. NMR spectroscopy has proved invaluable in the study of fast exchange-rate processes in both cyclic and acyclic molecules. Four techniques have been used to measure the exchange rates by NMR spectroscopy— namely, (1) the steady-state or high-resolution technique, (2) the spin-echo, (3) double-resonance, and (4) the fast-passage method, of which the first two are by far the most commonly used. The appearance of the high-resolution spectrum of an inverting molecule is governed by the rate of exchange and the internal chemical shift between nuclei in different sites. In the low-temperature spectrum, the high-field peak is due to the conformer with axial hydrogen and the low-field peak to the conformer with equatorial hydrogen. Later, the chapter discusses the validity of the karplus equation." @default.
- W896767401 created "2016-06-24" @default.
- W896767401 creator A5057132819 @default.
- W896767401 date "1968-01-01" @default.
- W896767401 modified "2023-10-15" @default.
- W896767401 title "Nuclear Magnetic Resonance Spectroscopy in Conformational Analysis" @default.
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