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- W897639765 abstract "Vanillin 1, 2-propylene glycol acetal was synthesized from vanillin and 1, 2-propylene glycol using H3PMo6W6O40•nH2O as catalyst. The factors influencing the synthesis were discussed and the better reaction conditions were found as follows: The amount of vanillin was 3.8 g, the molar ratio of vanillin was 1, 2-propylene glycol 1.0 to 2.4. the amount of catalyst was 1.6% in proportion to the total reacting materials, the volume of cyclohexane as the water-carrying agent 4 mL, the refluxing time was 2 h at 88-96℃ and thus the product yield reached over 87%. The results show that the catalyst's activity is high and the reaction time is short." @default.
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- W897639765 date "2010-02-25" @default.
- W897639765 modified "2023-09-26" @default.
- W897639765 title "Synthesis of Vanillin 1,2-Propylene Glycol Acetal Catalyzed by H3PMo6W6O40•nH2O" @default.
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