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- W906222772 abstract "The growth of LaBr3:Ce 3+ crystal by the vertical Bridgman process in a nonvacuum atmosphere was reported. According to the dehydration procedure of LaBr3·7H2O and CeBr3·7H2O investigated by differential thermal analysis/thermogravimetry (DTA/TG), anhydrous LaBr3 and CeBr3 were prepared by heating LaBr3·7H2O and CeBr3·7H2O at 240–260◦C for 5–6 h in dried HBr atmosphere. Using the feed materials prepared from the anhydrous lanthanon bromides, a 0.5 mole fraction Ce doped LaBr3 crystal with size of φ25 mm×50 mm had been grown by vertical Bridgman process successfully. By sealing the feed material in a platinum crucible, the crystal could be grown in a nonvacuum atmosphere as the oxidization and volatilization of the melt could be avoided. The crystal was grown with the optimum conditions such as a growth rate of 0.5–1.0 mm/h and a temperature gradient of around 30◦C/cm across solid-liquid interface under a furnace temperature of 850–880◦C. The crystal was characterized by DTA/TG, X-ray diffraction (XRD), optical transmission, photoluminescence and X-ray stimulated luminescence measurement. The Bridgman process was confirmed to be promising for growing transparent LaBr3:Ce 3+ crystal with high optical quality." @default.
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- W906222772 date "2009-11-24" @default.
- W906222772 modified "2023-09-28" @default.
- W906222772 title "Growth of LaBr3:Ce3+ single crystal by vertical Bridgman process in nonvacuum atmosphere" @default.
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