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- W917105802 abstract "１引言以纤维素酯制备的手性固定相（ＣＳＰ）主要在正相条件下被使用，然而对于一些酸性或碱性外消旋化合物由于在流动相中溶解困难等原因，在正相条件下难以直接进行拆分。Ｉｋｅｄａ等首先报道了纤维素－三（３，５－二甲基本基氨基甲酸酯）手性柱（ＯＤ）在反相条件下的应用。我们在自己制备的纤维素－三（苯基氨基甲酸酯）手性柱（ＣＴＰＣ）上，首次在反相条件下直接拆分了一系列酸性外消旋药物，说明ＣＴＰＣ柱在反相条件下同样具有较好的手性拆分能力。２实验部分２．１试剂 微晶纤维素（上海试剂二厂），异氰酸苯酯（Ａ．Ｒ．Ｍｅｒｃｋ，Ｇｅｒｍａｎｙ），其余所用试剂均为分析纯。水为二次去离子水．酸性外消旋药物由常俊标博士合成并" @default.
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- W917105802 date "1997-12-15" @default.
- W917105802 modified "2023-09-27" @default.
- W917105802 title "酸性外消旋药物在纤维素-三(苯基氨基甲酸酯)手性柱上的直接拆分" @default.
- W917105802 hasPublicationYear "1997" @default.
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