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- W92127815 abstract "LC-NMR utilizing (1)H and (29)Si NMR spectroscopy is ideally suited for the analysis of silicones. It is shown that reversed phase gradient LC-NMR surpasses standard gel permeation chromatography (GPC) and diffusion ordered spectroscopy (DOSY) in the analysis of model hydride terminated polydimethylsiloxane. (1)H and (29)Si NMR in the stopped-flow arrangement leads to full identification of the components. Concentration gradient introduces a dependence of the (29)Si shifts on solvent composition, this dependence can be substantially reduced by a proposed method of referencing. It is shown that the ADEQUATE version of powerful but insensitive 2D INADEQUATE experiment can be used for complete line assignment." @default.
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- W92127815 date "2007-03-01" @default.
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- W92127815 title "High-performance liquid chromatography with nuclear magnetic resonance detection applied to organosilicon polymers" @default.
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- W92127815 doi "https://doi.org/10.1016/j.chroma.2007.01.078" @default.
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