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• W923261355 abstract "In this work single phase hexagonal YMnO3 powders were prepared starting from Y(CH3COO)3·xH2O, Mn(CH3COO)2·4H2O, KMnO4 and KOH using methods of conventional (280 °C for 6 h) or microwave assisted hydrothermal synthesis (200 °C for 2 h) followed by calcination at 1200 °C for 2 h. According to FESEM analysis the calcined powders consisted of submicronic YMnO3 particles, which were uniform in shape and size. Ceramic samples were obtained by sintering the as-synthesized powders at 1400 °C for 2 h. XRD analysis confirmed the presence of the single phase hexagonal YMnO3. SEM analysis showed a dense and homogeneous microstructure with typical inter- and intra-grain cracks. Magnetic measurements indicated ferrimagnetic properties that were explained by non-stoichiometry of the obtained compound and an excess of manganese that was confirmed by ICP analysis." @default.
• W923261355 created "2016-06-24" @default.
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• W923261355 date "2015-12-01" @default.
• W923261355 modified "2023-10-18" @default.
• W923261355 title "Hydrothermally assisted synthesis of YMnO" @default.
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• W923261355 doi "https://doi.org/10.1016/j.ceramint.2015.07.060" @default.
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