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- W926499319 abstract "Two novel vic-dioxime, 1,2-dihydroxyimino-1-p-tolyl-3-aza-6-imidazole heptane (L 1 H 2 ) and N-(ethyl-4-amino-1-piperidine carboxylate)-p-tolylglyoxime (L 2 H 2 ) were prepared by the reaction of anti-p-tolylchloroglyoxime with 1-(3-aminopropyl)imidazole and ethyl-4-amino-1-piperidine carboxylate in absolute THF. Mononuclear complexes with a metal-ligand ratio of 1:2 were prepared using Co(II), Cu(II) and Ni(II) salts. The ligands and their Co(II), Cu(II) and Ni(II) complexes were characterized by elemental analyses, FT-IR, UV-Vis, 1 H-NMR and 1 3 C-NMR and magnetic susceptibility measurements. The electrochemical behaviour of the complexes was investigated by cyclic voltammetry in dimethylsulfoxide. All metal complexes showed metal centered quasi reversible one-electron redox processes. However, metal complexes of the L 2 H 2 ligand also exhibited ligand based irreversible redox waves." @default.
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- W926499319 date "2005-01-01" @default.
- W926499319 modified "2023-09-23" @default.
- W926499319 title "Synthesis, Characterization and Redox Properties of Novel vic-Dioximes and Their Complexes with Nickel(ii), Copper(II) and Cobalt(II)" @default.
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