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- W930338240 abstract "A stable Pd(Ⅱ) compound Pd(AETYF)Cl2·CH2Cl2 (AETYF=4′,5′-diaza-9′-(4,5-bis(ethylthio)-1,3-dithiole-2-ylidene)-fluorene) has been synthesized and its crystal structure was determined by X-ray crystallography. The crystal is of monoclinic, space group P21/c with a=15.249(6), b=8.619(3), c=19.078(7)A^°,β=106.932(8)°, C19H18Cl4N2PdS4, Mr=650.79, V=2398.6(16)A^°3, Z= 4, Dc=1.802 g/cm^3, F(000)=1296,μ=1.579mm^-1, Npar=268, the final R=0.0538 and wR=0.1282 for 5068 observed reflections withⅠ>2σ(Ⅰ). The crystal structure determi-nation shows that the atoms of the molecule, except two ethyl-groups, are conjugated in a quasiplane and these molecules are further stacked or contacted via plane to plane or edge to edge π-π interactions, forming parallel molecular chains along the b axis." @default.
- W930338240 created "2016-06-24" @default.
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- W930338240 date "2004-01-01" @default.
- W930338240 modified "2023-09-26" @default.
- W930338240 title "Synthesis and Crystal Structure of Pd（AETYF）CIe-CHeCl2 [AETYF=4′,5′-Diaza-9′（4,5-bis（ethylthio）- 1,3-dithiole-2-ylidene）-fluorene]" @default.
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