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- W93134653 abstract "A direct potentiometric titration method is described for the determination of chloride in the range of 0.005 to 0.15% in uranium-bearing feed materials. The titration is carried out to a predetermined equivalence potential in a 95% methanol--5% nitric acid medium. A silver wire-saturated calomel electrode system is used. The method is rapid, since no preliminary separation of the chloride is required. The major interferences for the titration are iron (III), vanadium (V), permanganate, nitrite, bromide, and iodide. The interference of all ions except bromide and iodide is prevented by the addition of ascorbic acid or ammonium hydroxide. A comparative study of the potentiometric and turbidimetric methods was made. Uranium ore concentrates, nitric acid, and aqueous feed samples were used in this study. Satisfactory agreement was obtained between the two methods, using these sample types. (auth)" @default.
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- W93134653 date "1958-11-01" @default.
- W93134653 modified "2023-09-27" @default.
- W93134653 title "DETERMINATION OF CHLORIDE IN URANIUM-BEARING MATERIALS BY A POTENTIOMETRIC TITRATION METHOD" @default.
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